Soft X-ray Spectroscopy of a Complex Heterojunction in High-Efficiency Thin-Film Photovoltaics: Intermixing and Zn Speciation at the Zn(O,S)/Cu(In,Ga)Se2 Interface

Document Type

Article

Publication Date

1-1-2016

Publication Title

ACS Applied Materials and Interfaces

Volume

8

Issue

48

First page number:

33256

Last page number:

33263

Abstract

The chemical structure of the Zn(O,S)/Cu(In,Ga)Se2 interface in high-efficiency photovoltaic devices is investigated using X-ray photoelectron and Auger electron spectroscopy, as well as soft X-ray emission spectroscopy. We find that the Ga/(Ga+In) ratio at the absorber surface does not change with the formation of the Zn(O,S)/Cu(In,Ga)Se2 interface. Furthermore, we find evidence for Zn in multiple bonding environments, including ZnS, ZnO, Zn(OH)2, and ZnSe. We also observe dehydrogenation of the Zn(O,S) buffer layer after Ar+ ion treatment. Similar to high-efficiency CdS/Cu(In,Ga)Se2 devices, intermixing occurs at the interface, with diffusion of Se into the buffer, and the formation of S - In and/or S - Ga bonds at or close to the interface. © 2016 American Chemical Society.

Keywords

alternative buffer layers; chalcopyrite thin-film solar cell; chemical structure; X-ray emission spectroscopy; X-ray photoelectron spectroscopy; Zn(O; S)

Language

English

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