Amine-Functionalized Polyglycidyl Methacrylate Microsphere as a Unified Template for the Synthesis of Gold Nanoparticles and Single-Crystal Gold Plates
Document Type
Article
Publication Date
3-25-2013
Publication Title
Macromolecular Rapid Communications
Volume
34
Issue
6
First page number:
504
Last page number:
510
Abstract
Polyglycidyl methacrylate (PGMA) microspheres, crosslinked and surface-functionalized by amine, can be used as a solid-state template for the synthesis of gold (Au) crystals in the forms of either nanoparticles (NPs) or plates. It is discovered that the polymer microsphere acts as an internal template to cultivate Au NPs inside the microsphere or an external template to generate the single-crystal plates depending on the critical concentration (Ccr) of gold ions. The ion–dipole interaction and the structure-dependent solubility of gold induce two distinct gold nanostructures in the presence of the functionalized polymer microspheres. The catalytic activity and long-term storage of the developed gold nanostructures that can be easily scaled-up for mass production through the developed novel methodology is demonstrated.
Keywords
Acrylates; Catalysts; Gold; Gold nanocrystals; Gold nanoparticles; Nanocrystals; Nanoparticles; Nanostructures; Polyglycidyl methacrylate; Polymer microspheres
Disciplines
Catalysis and Reaction Engineering | Chemical Engineering | Chemistry | Mechanical Engineering | Nanoscience and Nanotechnology
Language
English
Permissions
Use Find in Your Library, contact the author, or interlibrary loan to garner a copy of the item. Publisher policy does not allow archiving the final published version. If a post-print (author's peer-reviewed manuscript) is allowed and available, or publisher policy changes, the item will be deposited.
Repository Citation
Oh, J. S.,
Dang, L. N.,
Yoon, S. W.,
Lee, P. C.,
Kim, D. O.,
Kim, K. J.,
Nam, J. D.
(2013).
Amine-Functionalized Polyglycidyl Methacrylate Microsphere as a Unified Template for the Synthesis of Gold Nanoparticles and Single-Crystal Gold Plates.
Macromolecular Rapid Communications, 34(6),
504-510.